研究生: |
黃裕勝 Yu-Sheng Huang |
---|---|
論文名稱: |
碳氮化硼-奈米碳管與奈米鑽石及二硫化鉬多層結構奈米材料之超級電容特性探討 BCN-CNT with N-UNCD and MoS2 Multiple Layer Nanomaterials for Supercapacitor Studies |
指導教授: |
黃柏仁
Bohr-Ran Huang |
口試委員: |
周賢鎧
許正良 |
學位類別: |
碩士 Master |
系所名稱: |
電資學院 - 光電工程研究所 Graduate Institute of Electro-Optical Engineering |
論文出版年: | 2023 |
畢業學年度: | 111 |
語文別: | 中文 |
論文頁數: | 332 |
中文關鍵詞: | 奈米碳管 、碳氮化硼 、超奈米鑽石 、二硫化鉬 、超級電容 |
外文關鍵詞: | CNTs, BCN, UNCD, MoS2, supercapacitor |
相關次數: | 點閱:312 下載:0 |
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本研究探討了碳氮化硼-奈米碳管與奈米鑽石及二硫化鉬多層結構奈米材料之超級電容特性,並探討不同後處理方式對於碳氮化硼-奈米碳管之結構影響,後續利用氮氣退火的方式探討多層結構之變化及電化學特性。
此研究發現對於BCN-CNT以及N-UNCD來說,氮氣退火後處理是提升其電性量測之最佳方式,並可以將BCN-CNTNA之面積電容從4.87 mF/ cm-2提升至30.11 mF/cm-2,而重量電容則提升至26.3 F/g,且其循環穩定性在經過4000次後,仍能保持86.5%。將BCN-CNT與MoS2以及N-UNCD進行堆疊後,[MoS2 / BCN-CNT]NA雖然因為MoS2對於電解液之影響,導致其循環穩定性下降,但其面積電容可以提升至49.52 mF/cm-2;而[N-UNCD / BCN-CNT]NA則因為鑽石之導電性較差,使其面積電容下降,但卻因鑽石對電解液之惰性,使其在循環穩定測試經過4000次循環後,仍能保持90.2%。
最後,由於BCN-CNT之高導電性,使其在電化學量測方面有著極佳之表現,並透過與N-UNCD和MoS2的堆疊,使其提升面積電容,或是提高其循環穩定性,不管是何種方式,皆表明BCN-CNT具有優異之電化學性能。
This study investigates the supercapacitor properties of boron carbon nitride-nanotubes (BCN-CNT) with UNCD and MoS2 multilayered nanostructures. It also explores the structural effects of different post-treatment methods on BCN-CNT and investigates the changes in the multilayered structures and electrochemical properties using N2 annealing.
The study found that N2 annealing is the optimal post-treatment method for improving the electrical measurements of BCN-CNT and N-UNCD. It can increase the areal capacitance of BCN-CNTNA from 4.87 mF/cm-2 to 30.11 mF/cm-2, and the specific capacitance to 26.3 F/g. The cyclic stability remains at 86.5% even after 4000 cycles. When BCN-CNT are stacked with MoS2 and N-UNCD, the [MoS2 / BCN-CNT]NA structure exhibits an increased areal capacitance of 49.52 mF/cm-2. However, its cyclic stability decreases. On the other hand, the [N-UNCD / BCN-CNT]NA structure shows a decrease in areal capacitance. However, its cyclic stability remains at 90.2% after 4000 cycles.
In conclusion, BCN-CNT contributes to its excellent electrochemical performance. Additionally, by stacking BCN-CNT with N-UNCD and MoS2, its electrochemical characteristics can be further enhanced. In any scenario, BCN-CNT demonstrates outstanding electrochemical performance.
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