二硫化鉬(Molybdenum Disulfide, MoS2)為二維奈米層狀材料，具備良好之電催化性能及耐蝕穩定性，惟其二維結構及層間作用力使其易產生團聚現象，導致活性反應點位降低並抑制電催化活性反應。還原氧化石墨烯(Reduced Graphene Oxide, rGO)具高電子遷移率，且偕同二硫化鉬可提供良好分散作用，有效抑制二硫化鉬之團聚現象產生，冀能進一步優化SS316L電極之電催化及電導性能。高級氧化處理透過電化學機制建構汙廢水處理技術其兼具自保持之機能，於電-芬頓系統中，陰極電極佔有相當重要地位。本研究以電泳沉積法於SS316L電極表面製備氧化石墨烯(Graphene Oxide, GO)，後續以脫氧處理完成rGO之製備，再以電沉積法複合二硫化鉬塗層；實驗過程以田口方法進行製程參數調整，期望提升電極電催化性及抗腐蝕性能，進一步提升電-芬頓系統之Rh B染劑降解效能。
結果顯示，相較SS316L電極，以電泳沉積電壓 45 V、GO 還原溫度 450 ℃ 及電沉積時間 600 s所製備之MoS2/rGO/SS316L複合電極其電催化性能、電導率及抗腐蝕能性可獲得顯著提升，該電極具最低腐蝕電流0.019 μA/cm2，電極具最低片電阻 4.77 kΩ·sq，同時陰極系統可獲致最高Rh B染劑降解率77.58 %；相較於SS316L電極，陰極系統Rh B降解率提升約1.4倍。綜上，還原氧化石墨烯複合二硫化鉬可有效改善塗層之均勻性及增加材料穩定性，藉此產生較高之反應活性點促進電催化反應，此結果可提供高級氧化處理電極材料揀選之參考。

Molybdenum Disulfide (MoS2) is a two-dimensional nano-layered material which possess good electrocatalysis performance and corrosion resistance. However, its two-dimensional structure and interlayer force make agglomeration easily, leading to lower active sites and inhibiting electrocatalysis reactions. Reduced graphene oxide (rGO) has high electronic mobility, and it can eliminate the agglomeration of MoS2 to improve the electrocatalysis. Advanced oxidation processes (AOPs) construct wastewater treatment technology by electrochemical mechanisms, which has a function of self-reliance. In this study, rGO was prepared on surface of SS316L electrode by electrophoresis deposition, then MoS2 was compounded by electrodeposition. The Taguchi method is used to optimize the parameters of process, improving the electrocatalysis performance and corrosion resistance of electrode, to enhanceing Rh B removal rate in Electro-Fenton system.
The results show that compared with SS316L electrode, the electrocatalysis performance, conductivity, and corrosion resistance of MoS2/rGO/SS316L prepared with 45 V by electrophoresis deposition, GO reduction temperature of 450 ℃, and electrodeposition time of 600 s can be significantly improved. This electrode possesses the lowest corrosion current of 0.019 μA/cm2, the lowest resistivity of 4.77 kΩ·sq, and the cathode system exhibited the highest Rh B degradation rate of 77.58%. In summary, rGO compounded with MoS2 can effectively modify the uniformity of coating and increase stability of electrode further. In this way, a higher active site is generated to promote the electrocatalysis reaction. This result can provide a reference to select electrode in AOPs.

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