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研究生: 杜維剛
Wei-Kang Tu
論文名稱: 單晶藍寶石基板平面研光製程之研光盤分析與開發研究
Analysis and Development of Lap for Mono-Crystalline Sapphire Wafer Lapping Process
指導教授: 陳炤彰
Chao-Chang Chen
口試委員: 趙崇禮
Choung-Lii Chao
鍾俊輝
Chun-Hui Chung
學位類別: 碩士
Master
系所名稱: 工程學院 - 機械工程系
Department of Mechanical Engineering
論文出版年: 2013
畢業學年度: 101
語文別: 中文
論文頁數: 201
中文關鍵詞: 藍寶石晶圓研光摩擦力溫度複合式檢測系統樹酯銅鐵研光盤
外文關鍵詞: Mono-crystalline sapphire wafer, Lapping, Friction and temperature complex detection syste, Resin copper-iron Lap
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因應單晶藍寶石基板於固態照明(solid-state illumination)產業之大量需求,為提高藍寶石晶圓生產效率與加工品質,完善的晶圓平坦化製程建立有其必要性,而晶圓研光製程(Lapping)之研光品質的優劣影響了後段拋光所需製程時間與成本,本研究主要在研發新型研光盤並分析加工壓力、研光盤轉速製程參數和不同研光盤材質對研光的影響,由本研究建立之摩擦力與溫度複合式線上檢測系統(Friction and temperature complex detection system, FTCS),藉由材料移除率、摩擦力與溫度等性能及製程資料來調整製程參數,並用於研光終點檢測。由拋光實驗結果可得,改變加工壓力與研光盤轉速對於材料移除率的增益約可提升10.6%及38.6%,且使用金屬銅盤製程對於材料移除率的影響性較樹酯銅盤顯著。本研究另製作出樹酯銅盤及樹酯銅鐵盤以發展創新之固相反應輔助研光製程,所發展樹酯銅盤及樹酯銅鐵盤之研光盤用於藍寶石晶圓研光可達到1微米/分鐘之材料移除率,平均表面粗糙度Sa為7奈米-9奈米。本研究建立之FTCS系統與創新研光盤與製程研究成果可作為未來先進基板研拋光產業新製程開發。


Due to demand of mono-crystal sapphire wafers in solid-state illumination industry, sapphire wafer planarization process needs to be investigated to improve wafer production efficiency and quality. Diamond lapping is one critical process to reduce long polishing time of sapphire wafers. This study develops a friction and temperature complex detected system (FTCS) for prediction of effects induced by lapping process parameter and different kinds of lapping plates. Based on performance of material removal rate (MRR), coefficient of friction (COF), variation of temperature obtained by the FTCS, the lapping process parameter can be used to find the endpoint detection of lapping process. Experimental results of MRR have been improved as 10.6% and 38.6% by increasing lapping pressure and lapping plate speed. Moreover, a self-developed resin copper lap (RCL) has been fabricated for comparison of MRR and a resin copper-iron lap (RCFL) has been designed and fabricated for developing a solid-state reaction assisted lapping (SS-Lapping) process of the sapphire wafers in this study, MRR could achieve up to 1 µm/min and surface roughness Sa maintains 7nm to 9nm by such self-made RCL and RCFL. Furthermore, the FTCS and RCFL could be applied on future study to develop different lapping process of advanced wafer fabrication.

摘要 I ABSTRACT II 誌謝 III 目錄 V 圖目錄 IX 表目錄 XIX 符號表 XXII 專有名詞對照表 XXIV 第一章 緒論 1 1.1研究背景 1 1.2研究目的與方法 3 1.3論文架構 3 第二章 文獻回顧 6 2.1單晶藍寶石基板 6 2.2硬脆材料磨料破壞行為探討 10 2.3磨料及研光盤於研光平坦化製程之影響 15 2.3.1磨料於研光製程之影響 15 2.3.2研光盤於研光製程之影響 25 2.4摩擦力與溫度於晶圓平坦化製程探討 27 2.5填充物與樹酯複材之探討 31 2.6文獻回顧總結 36 第三章 研光平坦化與相關實驗原理介紹 38 3.1研光機制 38 3.1.1研光原理與加工模式 38 3.1.2固相反應(Solid-state reaction)輔助機械研光之方法 39 3.1.3 固相反應(Solid-state reaction)輔助機械研光材料移除機制 與製程之建立 41 3.1.4 Preston材料移除經驗公式(Preston Equation) 43 3.2研光平坦化材料移除機制與製程模型建立 46 第四章 實驗設備與規劃 50 4.1研光(LAPPING)與研光盤檢測系統 50 4.2實驗設備 51 4.3實驗耗材 51 4.3.1鑽石研光液 52 4.3.2研光盤 53 4.3.3鑽石修整器與研光盤平坦度量測儀 54 4.3.4研光盤開發用模具及烤爐 55 4.3.5單晶藍寶石晶圓(Sapphire Wafer) 56 4.3.6樹酯、硬化劑 58 4.3.7填充粉末 58 4.4量測設備 59 4.4.1摩擦力感測器 59 4.4.2紅外線即時溫度觀測系統 60 4.4.4CCI-Lite表面干涉儀 62 4.4.5掃描式電子顯微鏡 63 4.4.6 TMA 64 4.4.7 TGA 65 4.4.8拉伸試驗機 66 4.4.9雷射粒徑分析儀 66 4.4.10精密電子天秤 67 4.5實驗規劃 68 4.5.1研光盤之技術開發 70 4.5.2研光盤於研光平坦化製程影響分析 72 第五章 實驗結果與討論 74 5.1研光盤開發製作 75 5.1.1硬度與楊氏模數分析 75 5.1.2材料熱重量與熱膨脹性質分析 77 5.2摩擦力與溫度於研光製程分析 80 5.2.1下壓力、轉速於研光製程影響分析 80 5.2.2金屬銅與樹酯銅研光盤於研光製程影響分析 87 5.2.3樹酯基研光盤於研光製程影響分析 95 5.3研光品質分析 103 5.4綜合結果與討論 113 第六章 結論與建議 120 6.1結論 120 6.2建議 122 參考文獻 124 附錄A各製程綠光干涉儀之表面粗糙度 128 附錄B 各製程溫度與摩擦力關係圖 168 作者介紹 174

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