研究生: |
班達廷 Mohammad - Badaruddin |
---|---|
論文名稱: |
水蒸氣對低碳鋼與熱浸鋁化低碳鋼高溫氧化之影響 Effects of Water-Vapour on the High Temperature Oxidation of Low Carbon Steel and Hot-Dip Aluminized Steel |
指導教授: |
王朝正
C.J. Wang |
口試委員: |
朱瑾
J.P. Chu 鄭偉鈞 W.C. Cheng 開物 Wu Kai 李志偉 J.W. Lee 林招松 C.S. Lin |
學位類別: |
博士 Doctor |
系所名稱: |
工程學院 - 機械工程系 Department of Mechanical Engineering |
論文出版年: | 2011 |
畢業學年度: | 99 |
語文別: | 英文 |
論文頁數: | 177 |
中文關鍵詞: | low carbon steel 、oxidation resistance 、columnar structure 、pyramidal grain 、carbon deposition aluminized steel 、coating 、water-vapour |
外文關鍵詞: | low carbon steel, oxidation resistance, columnar structure, pyramidal grain, carbon deposition aluminized steel, coating, water-vapour |
相關次數: | 點閱:279 下載:5 |
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The oxidation kinetics of low carbon steel was studied in dry air, mixed steam, pure steam, and ethanol at the temperature range of 700800 °C after 49 h exposure at atmospheric pressure. Similar parabolic oxidation kinetics is observed for the steels exposed to dry air and mixed steam. The mass-gain data on the steel exposed to ethanol at 800 °C is similar to the mass-gain data on the steels exposed to pure steam at 700–800 °C having two stages of parabolic kinetics. The rates of steel oxidized in mixed steam at 700, 750 and 800 °C rises by a factor of 10.06, 2.58, and 2.84, respectively. The rate of steels oxidized in pure steam at 700, 750 and 800 °C rises by a factor of 4.64, 2.91, and 2.59, respectively and in ethanol the rate was respectively increased to 7.71, 1.37, and 2.08 at 700, 750 and 800 °C with respect to those oxidized in dry air. The activation energy is found to be lower (200 kJ/mol) in steel oxidized in ethanol than those of steels oxidized in dry air (318 kJ/mol), mixed steam (206 kJ/mol) and pure steam (266 kJ/mol). The carbon deposition in the magnetite layer gave rise to the breakaway oxidation in ethanol oxidation at 800 °C after about 9 h. In their cross sections, the scale has a columnar structure and appears two layers with a thin outer magnetite layer and an inner wustite layer in dry air and mixed steam whereas in pure steam and ethanol the scale structures show a thick magnetite layer and the thin wustite layer revealed very porous.
Low carbon steel, AISI 1005, was coated by hot-dipping into a molten Al-10%Si bath at 700 °C for 18 s. After hot-dipping treatment, the coating layers consisted of Al, Si, FeAl3, τ5-Fe2Al8Si, and Fe2Al5. After oxidation tests, the FeAl3 and τ5-Fe2Al8Si phases were completely transformed to the Fe2Al5 and FeAl2 in the alumnide layer, whereas the FeAl formed near the steel substrate was due to Fe-atoms diffusing into the Fe2Al5 layer when the time and temperature were increased.
Hot-dip aluminized AISI 1005 steel was isothermally oxidized at temperatures varying from 700 to 800 °C in air, mixed steam and pure steam at atmospheric pressure. The high-temperature steam resistance of aluminized steel depended on the oxidation temperature. It was shown that in atmospheres that contain water-vapour, the alumina formed on the surface coating had less protection than in a dry air atmosphere. The presence of water-vapour enhanced Fe-ion transport processes in the alumina due to the incorporation of hydrogen. The rapid growth of sporadic iron oxide nodules on the coating surface and at the interface was accelerated by rapid outward diffusion of Fe-ions; high-pressure H2 from water-vapour dissociation; and crack formation in the aluminide layer. Thus the oxidation rate was increased, resulting in a substantial mass-gain with temperature and time. In addition, the aluminum exhibited a greater tendency to become internally oxidized in a low pO2-steam than in a high pO2-steam.
Keywords: low carbon steel; oxidation resistance; columnar structure; pyramidal grain; carbon deposition; aluminized steel; coating; water-vapour.
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