本研究以嫘縈(Viscose Rayon) 針織物為原料，經95％的硫酸銨(AS)及5％磷酸氫二銨(AP)，濃度為30％之複合式耐燃劑前處理後，做為前驅體（Precursor）。利用一連續之直立式半開放高溫爐，經過氧化、碳化及活化工程，製作活性碳纖維布。實驗中利用不同碳化溫度600℃、700℃、800℃、900℃及1000℃，並改變活化源，來探討活性碳纖維布的微細結構與化學性質。
當碳化溫度越高，產率下降，而真密度與結晶厚度越大，其導電度亦隨之增加。當加入水與空氣為活化源時，比表面積增加，有機氣體吸附率上升。
結果顯示，所製備出的活性碳纖維以微孔結構為主，在水蒸氣加空氣當活化源所製備出之活性碳纖維，其比表面積達1411.6 m²/g，而其結構較緻密，結晶厚度為3.84，真實密度值2.59 g/cm³，對四氯化碳氣體吸附量為97.5%。

This study used viscose rayon-based knitted fabrics as raw materials and pretreated with composite flame retardant concentration of 30% of 95% AS and 5% AP to prepare the precursor. This nonstop vertical row semi-open high temperature furnace was employed to produce activated carbon fiber cloth after oxidation, carbonization, and activation. During the experiment, the micro structure and chemical properties of the activated carbon fiber cloth were explored and discussed by using different carbonization temperatures at 600℃, 700℃, 800℃, 900℃ and 1000℃ and changing activation sources.
When the carbonization temperature becomes higher, the production rate drops while the true density and crystallization thickness become greater with increasing electrical conductivity. When water or air was added as the source of activation, the specific surface area increased and the absorption rate of organic gases also rose.
The results showed that the produced activated carbon fiber was mainly of micro-porous structure. The activated carbon fiber prepared by using water vapor and air as the activation source had a specific surface area up to 1411.6 m²/g, and its structure was relatively dense with crystallization thickness at 3.84. The true density value was 2.59 g/cm³, and absorption rate of carbon tetrachloride was 97.5%.

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