本研究探討了碳氮化硼-奈米碳管與奈米鑽石及二硫化鉬多層結構奈米材料之超級電容特性，並探討不同後處理方式對於碳氮化硼-奈米碳管之結構影響，後續利用氮氣退火的方式探討多層結構之變化及電化學特性。

此研究發現對於BCN-CNT以及N-UNCD來說，氮氣退火後處理是提升其電性量測之最佳方式，並可以將BCN-CNTNA之面積電容從4.87 mF/ cm-2提升至30.11 mF/cm-2，而重量電容則提升至26.3 F/g，且其循環穩定性在經過4000次後，仍能保持86.5%。將BCN-CNT與MoS2以及N-UNCD進行堆疊後，[MoS2 / BCN-CNT]NA雖然因為MoS2對於電解液之影響，導致其循環穩定性下降，但其面積電容可以提升至49.52 mF/cm-2；而[N-UNCD / BCN-CNT]NA則因為鑽石之導電性較差，使其面積電容下降，但卻因鑽石對電解液之惰性，使其在循環穩定測試經過4000次循環後，仍能保持90.2%。

最後，由於BCN-CNT之高導電性，使其在電化學量測方面有著極佳之表現，並透過與N-UNCD和MoS2的堆疊，使其提升面積電容，或是提高其循環穩定性，不管是何種方式，皆表明BCN-CNT具有優異之電化學性能。

This study investigates the supercapacitor properties of boron carbon nitride-nanotubes (BCN-CNT) with UNCD and MoS2 multilayered nanostructures. It also explores the structural effects of different post-treatment methods on BCN-CNT and investigates the changes in the multilayered structures and electrochemical properties using N2 annealing.

The study found that N2 annealing is the optimal post-treatment method for improving the electrical measurements of BCN-CNT and N-UNCD. It can increase the areal capacitance of BCN-CNTNA from 4.87 mF/cm-2 to 30.11 mF/cm-2, and the specific capacitance to 26.3 F/g. The cyclic stability remains at 86.5% even after 4000 cycles. When BCN-CNT are stacked with MoS2 and N-UNCD, the [MoS2 / BCN-CNT]NA structure exhibits an increased areal capacitance of 49.52 mF/cm-2. However, its cyclic stability decreases. On the other hand, the [N-UNCD / BCN-CNT]NA structure shows a decrease in areal capacitance. However, its cyclic stability remains at 90.2% after 4000 cycles.

In conclusion, BCN-CNT contributes to its excellent electrochemical performance. Additionally, by stacking BCN-CNT with N-UNCD and MoS2, its electrochemical characteristics can be further enhanced. In any scenario, BCN-CNT demonstrates outstanding electrochemical performance.

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