可調控官能化碳基底複合膜用於水處理之研究｜國立臺灣科技大學博碩士論文系統

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研究生：	THAGARE MANJUNATHA SUBRAHMANYA THAGARE MANJUNATHA SUBRAHMANYA
論文名稱：	可調控官能化碳基底複合膜用於水處理之研究 Switchable Functionalized Carbon-based Composite Membranes for Water Treatment
指導教授：	洪維松 Wei-Song Hung
口試委員:	Juin-Yih Lai Juin-Yih Lai Chien-Chieh Hu Chien-Chieh Hu Chih-Feng Wang Chih-Feng Wang Da Ming Wang Da Ming Wang Shiao-Wei Kuo Shiao-Wei Kuo Tai-Shung Chung Tai-Shung Chung
學位類別：	博士 Doctor
系所名稱：	應用科技學院 - 應用科技研究所 Graduate Institute of Applied Science and Technology
論文出版年：	2022
畢業學年度：	110
語文別：	英文
論文頁數：	175
中文關鍵詞：	薄膜蒸餾、石墨烯、海水淡化、聚偏氟乙烯、奈米碳管、染料去除、能源效率、注射器過濾、智能薄膜
外文關鍵詞：	Membrane distillation, Graphene, Desalination, PVDF, CNTs, Dyes removal, energy efficiency, syringe filtration, smart membranes
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上一筆

近年來，智能聚合物奈米複合膜由於接觸不同外在條件時能夠轉換膜的特性，使其可用於包括水處理在內的各種應用而被熱切的關注著。在本論文中，我們首先展示了石墨烯-PVDF平板膜在海水淡化中「自加熱VMD模式」下的表面熱傳導。該系統消除了 TP 並在脫鹽方面表現出高性能（即 Qsh= 0.109 kWh/L，GOR= 5.72，Flux= 23.44 L/m2h 和脫鹽率= 99.41 %）。我們還進行了 FVM 模擬以驗證實驗結果。在第二項研究中，我們製造了一種新型流動式原位蒸發薄膜 (FTIEM)，用於長時間VMD 模式的海水淡化。FTIEM (COOH-MWCNTs-PVA) 的中間層為網狀式熱傳導層，在其頂部塗有 PEI-PDA-SBA-15 以用作水合、鹽屏蔽和隔熱層。然而，蒸汽被PVDF 膜（FTIEM 的底層）選擇性的傳輸。因此，我們在 MD 過程中實現了最低的 Qsh (0.024 kWhL-1) 和長期穩定性，通量和脫鹽率分別為 29.25 Lm-2h-1 和 99.99%，使其成為最具吸引力的海水淡化方案。在第三項研究中，我們開發了用於注射器中能去除染料的 GO/(SBA-15/PDA)複合過濾薄膜。我們發現 GO10/(SBA-15/PDA)2 的效能是最佳的（MB 的滲透通量為2487.4 Lm-2h-1b-1、去除率為 99.61%，而EBT的滲透通量為2486.4 Lm-2h-1b-1、去除率為 90.86%），在很大的 pH 範圍內表現出良好的穩定性和性能。pH 值的變化起到了關鍵作用，增強了染料和膜之間的靜電吸引力。這種膜在處理染料廢水方面具有很大的潛力。總體而言，這些研究為新一代的智能薄膜開闢了新途徑。

In recent years, smart polymer nanocomposite membranes have gained great interest due to their ability to switch properties when exposed to external trigger, making them useful for various applications, including water treatment. In this dissertation, we first demonstrated Graphene-PVDF flat sheet membrane for interfacial joule heating in self- heated VMD mode of sea water desalination. The system eliminated TP and showed high performance in desalination (i.e., Qsh= 0.109 kWh/L, GOR= 5.72, Flux= 23.44 L/m2h and salt rejection= 99.41 %). Also we performed FVM simulation to validate with the experimental results. In the second study, we fabricated a novel flow-through in-situ evaporation membranes (FTIEMs) for long term VMD mode of hypersaline water desalination. The middle layer of FTIEM (COOH-MWCNTs-PVA) was deployed as joule heating network, on top of it PEI-PDA-SBA-15 was coated to serve as hydrating, salt screening as well as thermally insulating layer. Whereas, PVDF membrane (bottom layer of FTIEM) was deployed for selective vapor transport. As a result, we achieved the lowest Qsh (0.024 kWhL-1) and long term stability during MD process with flux and salt rejection of 29.25 Lm-2h-1 and 99.99% respectively, offering it to be the most attractive solution for desalination. In the third study, we developed GO/(SBA-15/PDA) composite syringe filter membranes for dyes removal. We found that the GO10/(SBA-15/PDA)2 was the optimum one (99.61 % removal with 2487.4 Lm-2h-1b-1 permeation flux for MB and 90.86 % removal with 2486.4 Lm-2h-1b-1 permeation flux for EBT), that exhibited good stability and performance over wide range of pH. The pH variation enhanced electrostatic attraction between dyes and the membrane played the key role. This membrane has great potential for the treatment of dye wastewater. Overall, these research works open new avenues for the development of a new generation smart membranes.

ABSTRACT    I
摘 要    III
CERTIFICATE    IV
DECLARATION    V
ACKNOWLEDGEMENT    VI
TABLE OF CONTENTS    VIII
LIST OF FIGURES    XII
LIST OF TABLES    XXI
LIST OF ABBREVIATIONS    XXIII
CHAPTER I INTRODUCTION    1
1    INTRODUCTION    2
2 DISSERTATION GOALS AND OUTLINE    6
CHAPTER II LITERATURE REVIEW    8
1 BACKGROUND OF MEMBRANE SCIENCE AND TECHNOLOGY    9
2 INTRODUCTION TO MEMBRANE SCIENCE AND TECHNOLOGY    11
3 PRESSURE DRIVEN MEMBRANE PROCESSES FOR WATER TREATMENT    12
4 THERMALLY DRIVEN MEMBRANE PROCESSES FOR WATER TREATMENT    13
5 CONVENTIONAL MD CONFIGURATIONS    15
5.1 Direct contact membrane distillation (DCMD)    15
5.2 Vacuum membrane distillation (VMD)    16
5.3 Air gap membrane distillation (AGMD)    16
5.4 Sweeping gas membrane distillation (SGMD)    16
6 TRADITIONAL MEMBRANES FOR PRESSURE AND THERMAL DRIVEN WATER TREATMENT    17
6.1 Inorganic membrane materials    18
6.2 Polymeric membrane materials    18
7 SMART POLYMER NANOCOMPOSITE MEMBRANES FOR WATER TREATMENT    19
8 SELF-HEATING MEMBRANES FOR WATER TREATMENT AND THEIR WORKING PRINCIPLES    22
8.1 Photothermal membranes    22
8.2 Induction heating membranes    23
8.3 Joule heating membranes    24
CHAPTER III High performance self-heated membrane distillation system for energy efficient desalination process    25
1 INTRODUCTION    26
2 EXPERIMENTAL    29
2.1 Materials    29
2.2 Fabrication of Graphenex-PVDF1 flat sheet membrane joule heaters    30
2.3 Preparation of PDMS treated PET nonwoven support layer for Graphenex –PVDF1 flat sheet membrane joule heaters.    30
2.4 Membrane characterization    31
2.5 Determination of Bulk porosity (%) and liquid entry pressure (LEP).    32
2.6 Experimental set up.    33
2.7 Simulation    36
2.8 Polynomial response surfaces with respect to the VMD experimental variables:    37
2.9 Determining the optimal temperature such that the difference between the ratio of the effective heating area of membrane and the ratio of pure water flux was minimized:    38
3 RESULT AND DISCUSSION    39
3.1 Morphological characterization of Graphenex-PVDF1 flat sheet membrane joule heaters    40
3.2 Physicochemical Characterization of Graphenex-PVDF1 flat sheet membrane joule heaters    43
3.3 Characterization of PDMS treated PET nonwoven support layer    51
3.4 Characterization of Few-layer graphene used in the fabrication of membrane joule heaters:    53
3.5 Self-heated VMD desalination performance of Graphenex-PVDF1 flat sheet membrane joule heaters    54
3.6 Simulation    63
3.7 SUMMARY    65
CHAPTER IV Flow-through in-situ evaporation membrane enabled self-heated membrane distillation for efficient desalination of hypersaline water    67
1 INTRODUCTION    68
2 EXPERIMENTAL    69
2.1 Materials    69
2.2 Fabrication of FTIEMs    70
2.3 Materials characterization    71
2.4 FTIEMD experiments    72
3 RESULT AND DISCUSSION    74
3.1 Morphological and physico-chemical characterization of SBA-15 and PEI-PDA-SBA-15    75
3.2 Morphological characterization of FTIEMs    78
3.3 Physico-chemical characterization and thermographic investigations of FTIEMs    82
3.4 FTIEMD performance    89
4 SUMMARY    96
CHAPTER V An eco-friendly and reusable syringe filter membrane for the efficient removal of dyes from water via low pressure filtration assisted self-assembling of Graphene Oxide and SBA-15/PDA    98
1 INTRODUCTION    99
2 EXPERIMENTAL    101
2.1 Materials and methods    101
2.2 Synthesis of SBA -15/PDA composite powder    102
2.3 Fabrication of GO/(SBA-15/PDA) syringe filter membranes    103
2.4 Characterization    104
2.5 Permeate flux and dye removal    105
2.6 Sorption performance of GO/(SBA-15/PDA) syringe filter membranes    106
2.7 Cyclic stability study of GO/(SBA-15/PDA) syringe filter membranes    106
2.8 Effect of pH    106
3 RESULT AND DISCUSSION    107
3.1 Morphological and physico-chemical characterization of SBA-15 and SBA-15/PDA composite    107
3.2 Morphological and physico-chemical characterization of GO/(SBA-15/PDA) Syringe filter membranes    109
3.3 Performance study of the GO/(SBA-15/PDA) syringe filter membranes.    115
4 SUMMARY    128
CHAPTER VI CONCLUSIONS AND FUTURE PERSPECTIVE    130
1 CONCLUSIONS    131
2 FUTURE PERSPECTIVE    133
3 LIST OF PUBLICATIONS    134
4 ACHIEVEMENTS    138
REFERENCES    138
                                

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