研究生: |
何宗育 Czung-Yu Ho |
---|---|
論文名稱: |
利用紫外光致相分離原理製作液晶分子垂直配向共聚薄膜及其光電特性探討 Fabrication of Vertical Alignment Composite Film (VACOF) for Liquid Crystal Molecules by Ultra-Violet Light Induce Phase Separation Principle and Their Electro-Optical Characteristics |
指導教授: |
李俊毅
Jiunn-Yih Lee |
口試委員: |
邱顯堂
none 邱士軒 none 張豐志 none 陳志勇 none 吳勛隆 none 鄭功龍 none |
學位類別: |
博士 Doctor |
系所名稱: |
工程學院 - 材料科學與工程系 Department of Materials Science and Engineering |
論文出版年: | 2011 |
畢業學年度: | 99 |
語文別: | 中文 |
論文頁數: | 212 |
中文關鍵詞: | 光電特性 、垂直配向共聚薄膜 、預聚物 、液晶 、非接觸 、電誘導分子傾斜角效應 |
外文關鍵詞: | Electro-Optical characteristic, Vertical alignment copolymer film, Pre-polymer, Liquid crystal, Non-contact, Electroclinic effect |
相關次數: | 點閱:485 下載:7 |
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本研究主要是利用非接觸光聚合誘發液晶(Liquid crystal, LC)與預聚物(Pre-polymer)產生其相分離行為後,以形成具有垂直配向效果的擬-聚合物(Polymer)薄膜。而在分子結構設計方面,我們採用具有烷基長碳鏈(Alkyl long carbon chain)和主鏈雙酚型(Main chain biphenol type)等光硬化壓克力預聚物(Photo-curable acrylic pre-polymer)並摻混光起始劑(Photo-initiator)以及負誘電異方型液晶(Negative dielectric anisotropy type liquid crystal, NLC)等成份,經充分攪拌與超音波震盪形成均一的液晶混合溶液(NLC/photo-curable acrylic pre-polymer mixture systems)。我們最初的構想是希望將此液晶混合溶液在經由紫外光(Ultra-violet, UV)照射後,因光聚合誘發相分離(Photo-polymerization induced phase separation, PIPS),使得NLC與photo-curable acrylic pre-polymer產生複合層化結構之垂直配向共聚薄膜(Vertical alignment copolymer film, VACOF)。而此新穎的光配向技術不僅可改善傳統摩擦(Rubbing)配向製程所產生的缺點以提升其良率之外,我們也期盼朝著製程縮短化以及面板低價化之目標邁進。
而本論文主要分為三大實驗系統。首先,我們主要探討此負型液晶/壓克力預聚物混合系統的光配向機制以及觀察液晶分子在不同碳鏈長度的烷基壓克力預聚物A之改變下,以量測液晶元件(LC device)的對比度(Contrast ratio)、光穿透度(Transmittance)以及反應時間(Response time)等光電特性(Electro-Optical characteristic)。而後,經由儀器量測出來的結果,如閥電壓(Threshold voltage, Vth)、驅動電壓(Driving voltage, Von)、飽和電壓(Saturation voltage, Vsat)以及反應時間等,我們大致可以推測其系統所生成之VACOF表面的錨定能(Anchoring energy)及其液晶分子的配向機制,藉以觀察對於不同碳鏈長度的烷基壓克力預聚物與液晶分子之間的相互作用力等關係。其次則是針對不同長度的主鏈雙酚型壓克力預聚物B之分子結構與液晶試片厚度(2 μm, 4 μm and 6 μm)下,對於VACOF表面微結構的影響、液晶元件的顯示情形以及光電特性等進行量測分析與探討。最後,我們希望藉由本實驗室所合成的雙旋光性液晶(Two chiral centres smectic A phase, SmA*)在摻入光致垂直配向之負型液晶/壓克力預聚物混合系統後,藉以達到輔助液晶分子整體垂直排列效果為其實驗之主要目的之一(SmA*液晶在正交偏光顯微鏡下為呈現垂直排列的紋理(Homeotropic texture))。另外,由於SmA*液晶本身具有電誘導分子傾斜角效應(Electroclinic effect),擁有比鐵電性(Ferroelectric)液晶還要快的反應時間,如此具有其快速應答、記憶性以及擁有可調變光線通過之灰階等特性。因此,我們希望藉由這些優點能夠改善原系統之光電性質。
In the study, we use non-contact photo-polymerization induced liquid crystal (LC) and pre-polymer to form a vertical alignment (VA) effect of pseudo-Polymer thin film after the phase separation. In the molecular structure design, we utilize photo-curable acrylic pre-polymer, (alkyl long carbon chain and main chain biphenol type etc.) and mix photo-initiator and negative dielectric anisotropy type liquid crystal (NLC) etc. component together. Forming the homogeneous LC mixture solution (NLC/photo-curable acrylic pre-polymer mixture systems) is via enough stirred and ultrasonic vibration. We use photo-polymerization induced phase separation (PIPS) effect, and to make the NLC and the photo-curable acrylic pre-polymer generate composite layer structure of the vertical alignment copolymer film (VACOF) after the Ultra-Violet (UV) light irradiation. The photo alignment of this novel technology can not only improve the traditional rubbing alignment shortcoming but also promote yield of the process. Our goal is expecting toward shortening the process for manufacture and decreasing the cost of the panel.
This paper was mainly divided into three experimental systems. First of all, we discussed the photo-alignment mechanism for the negative-type LC/acrylic pre-polymers mixture systems and measured electro-optical characteristic of the LC device, such as the contrast ratio, transmittance, response time etc. of the LC molecules under variant carbon chain length of alkyl acrylic photo-alignment A. By the quantitative data such as threshold voltage (Vth), driving voltage (Von), saturation voltage (Vsat) and reaction time and so on, we could extrapolate the anchoring energy of VACOF surface in this systems, the photo-alignment mechanism of LC molecules and the interaction between the acrylic pre-polymers of different alkyl chain length and the LC molecules and so forth. Secondly, we analyzed and discussed the influence on VACOF surface micro-structure, LC device’s display conditions and electro-optical properties in the molecule structure of main chain bisphenol type acrylic pre-polymers B of different length and the LC cell of different thickness (2 μm, 4 μm and 6 μm). Finally, we expect to arrange overall LC molecules in a vertical alignment by mixing two chiral centres smectic A (SmA *) LC synthesized in our laboratory with photo-induced vertical alignment negative type LC/acrylic pre-polymer mixture systems. (SmA* LC resulted in a homeotropic texture under the POM with crossed polarizers). In addition, due to the SmA* LC exhibits the electrical field induced molecular tilt effect (electroclinic effect) and offers faster response time than ferroelectric LC, it has the characteristics of fast response and memory, and further allows for the gray-scale capability of adjusting the amount of light passing through etc. We hope to take advantage of the SmA* LC materials to improve electro-optical characteristics of the original system.
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