光滑注液多孔表面（SLIPS）是一種由潤滑的微/納米結構與油構成的表面。
這種固被固定的潤滑劑有效創造出一個超光滑、連續的和化學上均勻的液
體表面，防止外來液滴直接接觸底層固體基質。各種研究表明，SLIPS 可
以降低結冰的速度，在高濕度的環境條件下有效地去除冷凝的水蒸氣，並
顯示出比超疏水表面（SHS）更低的冰附著力。SLIPS 點燃了塗層技術創
新的新方法，包括醫療設備的表面塗層、提高抗凍性的表面塗層、防垢和
防腐蝕。在這篇論文中，為了提高 SLIPS 的環境友好性、防水性和穩定性，
設計並通過 PVD 磁控濺射工藝製備了金屬奈米管陣列（MeNTAs）。然後
選擇 Kritox GPL103、Kritox GPL105 和 Kritox GPL107 三種油來潤滑
MeNTAs 使之成為 MeNTAs SLIPS。通過掃描電子顯微鏡（SEM）觀察了
MeNTAs 和 MeNTAs SLIPS 的結構。利用接觸角分析儀對 MeNTAs SLIPS
的潤濕性進行了鑑定，並研究了 MeNTAs SLIPS 的超光滑特性、耐久性和
抗冰性能。結果表明，使用直流磁控濺鍍方法成功地制造了直徑為 1、2、
10和20微米、高2微米的Zr-Cu-Al-Ni MeNTAs，它們具有良好的疏水性，
WCA 高於 110°。製造出的 MeNTAs SLIPS 具有良好的疏水性，WCA 高於
90，MeNTAs SLIPS GPL103、MeNTAs SLIPS GPL105 和 MeNTAs SLIPS
GPL107 的平均 WCA 分別為 116°、101°和 95°。此外，MeNTAs SLIPS
GPL103 出現了強力的水吸附性，而 MeNTAs SLIPS GPL105 和 MeNTAs
SLIPS GPL107 的 WSA 非常低，為 0.5°。MeNTAs SLIPS 顯示出延遲結冰
vi
的特性，可以在 24 次結冰周期內保持 WCA 穩定。與 MeNTAs SLIPS
GPL103 和 MeNTAs SLIPS GPL105 相比，MeNTAs SLIPS GPL107 顯示出
最佳性能。結果表明，小直徑的 MeNTAs 比大尺寸的表現更好。MeNTAs
SLIPS 在高速旋轉耐久測試中顯示出穩定的疏水性，MeNTAS SLIPS
GPL105 和 MeNTAS SLIPS GPL107 的 WSA 分別低於 7.2°和 2.1°。SEM 圖
像顯示了結冰和除冰過程對 MeNTAs 結構造成的損害。

Slippery Liquid-Infused Porous Surface (SLIPS) is a surface that comprises a
lubricating micro/nano-structured substrate with oil. This immobilized lubricant efficiently
creates an ultra-smooth, continuous, and chemically homogenous liquid surface, preventing
foreign liquid droplets from directly contacting the underlying solid substrate. Various studies
have shown that SLIPS can reduce the rate of ice accretion, effectively remove condensed water
vapor in high humidity environmental conditions, and shows a lower adhesion to ice than
superhydrophobic surface (SHS). SLIPS has ignited new methods of innovation in coating
technologies, including surface coatings on medical devices, surface coatings to improve frost
resistance, anti-scaling, and anti-corrosion. In this thesis, to improve environmental friendly,
the water-repellency and stability of SLIPS, Metallic Nanotube Arrays (MeNTAs) was
designed and prepared through a PVD magnetron sputtering process. Then three kind of oils,
Kritox GPL103, Kritox GPL105, and Kritox GPL107 oil, were selected to lubricate MeNTAs
become MeNTAs SLIPS. The MeNTAs and MeNTAs SLIPS structures were observed by
scanning electron microscopy (SEM). The wettability characteristic of MeNTAs SLIPS was
characterized by contact angle analyser and slippery characteristic, durability and anti-icing
properties of MeNTAs SLIPS were studied. The result shows that Zr-Cu-Al-Ni MeNTAs with
sizes 1, 2, 10, and 20 µm in diameter and 2 µm high was successfully fabricated using the
DCMS methods, they have good hydrophobicity with WCA above 110°. The fabricated
MeNTAs SLIPS produce SLIPS with good hydrophobicity characterized by WCA above 90,
MeNTAs SLIPS GPL103, MeNTAs SLIPS GPL105 and MeNTAs SLIPS GPL107, have an
average WCA of 116°, 101°, and 95 °, respectively. Furthermore, MeNTAs SLIPS GPL103
experienced water pinning, while MeNTAs SLIPS GPL105 and MeNTAs SLIPS GPL107 had
very low WSA of 0.5°. MeNTAs SLIPS show ice delaying characteristics and can maintain
WCA stable up to 24 times icing cycles. MeNTAs SLIPS GPL107 showed the best performance
compared to MeNTAs SLIPS GPL103 and MeNTAs SLIPS GPL105. And the result show that
small diameter MeNTAs perform better than the big size ones. MeNTAs SLIPS show stable
hydrophobicity at spinning test that showed WSA below 7.2° and 2.1° for MeNTAS SLIPS
GPL105 and MeNTAS SLIPS GPL107, respectively. SEM Images showed damage to the
structure of MeNTAs caused by the icing and deicing process.

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