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研究生： 陳松郁
Song-Yu Chen
論文名稱： 以龍捲式常壓電漿驗證石墨氈電極之電漿-基板交互作用於釩液流電池電性能提升
Elucidating the Plasma-Substrate Interaction on Graphite Felt Electrode Using Tornado-Type Atmospheric Pressure Plasma Jet and Its Improvement in the Vanadium Redox Flow Batteries
指導教授： 郭俞麟
Yu-Lin Kuo
口試委員: 王冠文
Kuan-Wen Wang
周昭昌
Chau-Chang Chou
洪逸明
I-Ming Hung
林長華
Chang-Hua Lin
王丞浩
Chen-Hao Wang
學位類別： 博士
Doctor
系所名稱： 工程學院 - 機械工程系
Department of Mechanical Engineering
論文出版年： 2023
畢業學年度： 111
語文別： 中文
論文頁數： 164
中文關鍵詞： 全釩氧化還原液流電池 、石墨氈電極 、潤濕性 、龍捲式常壓電漿噴射束 、官能化
外文關鍵詞： Vanadium Redox Flow Battery (VRFB), Graphite felt electrode, Wettability, Tornado-type Atmospheric Pressure Plasma Jet (APPJ), Functionalization
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    • 第一章 簡介..........1 1.1 前言..........1 1.2 研究目的與動機..........4 第二章 文獻回顧..........5 2.1 全釩液流電池概述..........5 2.2 全釩液流電池反應機制..........6 2.3 全釩液流電池架構介紹..........8 2.4 全釩液流電池之電極..........9 2.4.1 碳纖維..........11 2.4.2 聚丙烯腈 (Polyacrylonitrile, PAN)..........11 2.4.3 PAN電極的選用..........14 2.5 官能化電機之反應機制電極之優勢..........15 2.5.1 高溫處理技術..........17 2.5.2 酸性藥劑..........19 2.5.3 催化物技術..........21 2.5.4 元素摻雜技術..........25 2.6 電漿原理..........27 2.6.1 電漿生成及基本反應..........28 2.6.2 湯森放電理論 (Townsend discharge theory)..........29 2.6.3 帕邢定律 (Paschen's law)..........30 2.6.4 電漿解離機制..........31 2.6.5 電漿的用途..........33 2.7 常壓電漿概述..........33 2.7.1 介電質屏障放電 (Dielectric Barrier Discharge, DBD)..........34 2.7.2 電暈放電 (Corona Discharge)..........34 2.7.3 電漿火炬 (Plasma Torch)..........35 2.7.4 常壓噴射式電漿 (Atmospheric Pressure Plasma Jet, APPJ)..........36 2.8 電漿-介面反應機制..........37 2.9 常壓電漿針對石墨氈進行改質..........39 第三章 實驗材料與方法..........41 3.1 研究設計..........41 3.2 實驗耗材..........43 3.3 實驗儀器與參數..........44 3.3.1 常壓電漿 (Atmospheric pressure plasma jet, APPJ)..........44 3.3.2 光學放射光譜儀(Optical Emission Spectroscopy, OES)..........45 3.3.3 場發射掃描式電子顯微鏡 (Field Emission Scanning Electron Microscope, FE-SEM)..........46 3.3.4 水滴接觸角量測儀 (Water contact angle, WCA)..........47 3.3.5 紅外線熱影像儀 (Thermographic camera or infrared camera)..........48 3.3.6 電化學分析儀..........49 3.3.7 熱電偶 (Thermocouple)..........50 3.3.8 拉曼光譜儀 (Raman spectroscopy)..........51 3.3.9 X射線光電子能譜儀 (X-ray photoelectron spectroscopy, XPS)..........52 第四章 結果與討論..........53 4.1 空氣電漿對石墨氈電極纖維之影響..........53 4.1.1 石墨氈電極熱裂解溫度量測..........53 4.1.2 電漿氣體溫度與電漿/基材接觸溫度量測..........54 4.1.3 空氣電漿內部物種分析..........57 4.1.4 空氣電漿與石墨氈電極接觸後之尾氣量測..........61 4.1.5 石墨氈電極纖維之表面形貌..........63 4.1.6 石墨氈電極之水滴接觸角與半電池電解液浸泡測試..........65 4.1.7 石墨氈電極之時效測試..........67 4.1.8 石墨氈電極於全電池專用電解液之接觸角測試與時效測試..........70 4.1.9 石墨氈電極之缺陷分析..........73 4.1.10 石墨氈電極之表面化學鍵結分析..........76 4.1.11 石墨氈電極之CV循環測試..........84 4.1.12 石墨氈電極之阻抗測試..........88 4.1.13 於不同掃描次數處理的石墨氈電極之全電池專用電解液接觸角與時效測試..........90 4.1.14 於不同掃描次數處理的石墨氈電極之CV循環測試..........93 4.1.15 於不同掃描次數處理的石墨氈電極之阻抗測試..........97 4.1.16 石墨氈電極於全電池性能與長時間充放電測試..........99 4.1.17 空氣電漿與石墨氈電極之介面反應機制推導..........105 4.2 氮氣、氮氣/氫氣混合氣之電漿氣氛效應對石墨氈電極電性之影響..........108 4.2.1 電漿氣體溫度與電漿/基材接觸溫度量測..........108 4.2.2 電漿內部物種分析..........110 4.2.3 電漿與石墨氈電極接觸之尾氣分析..........114 4.2.4 石墨氈電極之表面形貌..........116 4.2.5 石墨氈電極之水滴接觸角與半電池電解液浸泡測試..........118 4.2.6 石墨氈電極之時效測試..........120 4.2.7 石墨氈電極於全電池專用電解液之接觸角與時效測試..........123 4.2.8 石墨氈電極缺陷分析..........126 4.2.9 石墨氈電極化學鍵結分析..........128 4.2.10 氮氣、氮氣/氫氣混合氣電漿處理之石墨氈電極循環測試..........132 4.2.11 石墨氈電極阻抗測試..........137 4.2.12 石墨氈電極全電池測試與長循環測試..........139 4.2.13 石墨氈電極之介面反應機制推導..........145 第五章 結果與討論..........149 第六章 未來展望..........151 參考文獻..........153

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